Record no |
201103224210 |
Activity status |
Dead or Administration by others |
Working Title |
A PROCESS FOR PREPARING THERMOTROPIC LIQUID CRYSTALLINE ELASTORMERS. |
Working Inventors |
SONPATKI MM;PORANATHNAM S;MASHELKAR RA; |
Contributing institutions |
NCL |
Administered by |
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Ownership |
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Categories > Subjects |
Polymer sciences and engineering |
Categories > Portfolio |
Polymers for speciality applications |
Disclosure number |
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NCL No |
1992-NCL-0015 |
CSIR No |
1992-NF-0128
|
Priority date |
12-03-1992 |
Country |
IN |
Application number |
1147DEL1992 |
Provisional filing date |
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Complete filing date |
12-03-1992 |
Publication status |
Yes |
Publication date |
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Publication no |
|
Granted number |
185918 |
Granted date |
12-14-2001 |
Final title |
A PROCESS FOR PREPARING THERMOTROPIC LIQUID CRYSTALLINE ELASTORMERS. |
Final Inventors |
SONPATKI MM;PORANATHNAM S;MASHELKAR RA; |
Abstract |
A process fAT tthe preparation of Thennotroplc Liquid
Crystalline gftlcTfJomprlses reacting Terephthaloyl Chloride
TPC with a poly alkylene glycol such as her In
described slowly raising the temperature of reaction form
60 90 C during a period of three hours with stirring
removing the hydrogen chloride formed by conventional
scrubbing adding Hydroqulnone HQ or Substituted Hydro
ulnone to the reaction mixture after the evolution of
hydrogen chloride Is stopped wherein ratio of TPC said
glycol HQ is 1 1 and glycol to HQ ratio ranges from
0.05 0.95 to 0.5 0.5 gaising the temperature of the
reaction mixture to 200 c gradually during a period of
three hours with stirring maintaining the reaction mixture
at this temperature for a period of 15 minutes.
purifying the polymer obtained by extraction with petroleum
e ther washing sequentially with 5 wtHtj ayqijecjua SQdlum
• .i te carbonate and water and then drying at a temperature of 100°C
Reference has been made to CopendIng Application o.1149 0 92 |
Case status |
Granted + Allowed to lapse |
Licensing status |
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Licensing case no |
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Client name |
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Lead inventors |
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Categories > Industry > Primary |
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Categories > Industry > other |
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